Extraction of Chlorophyll From Technologically Prepared Spinach Leaves

  IJETT-book-cover  International Journal of Engineering Trends and Technology (IJETT)          
  
© 2021 by IJETT Journal
Volume-69 Issue-4
Year of Publication : 2021
Authors : A. Kh-Kh. Nugmanov, I.Yu. Aleksanyan, M.A.S. Barzola, L.M. Titova, Z.M. Arabova
DOI :  10.14445/22315381/IJETT-V69I4P215

Citation 

MLA Style: A. Kh-Kh. Nugmanov, I.Yu. Aleksanyan, M.A.S. Barzola, L.M. Titova, Z.M. Arabova  "Extraction of Chlorophyll From Technologically Prepared Spinach Leaves" International Journal of Engineering Trends and Technology 69.4(2021):100-106. 

APA Style:A. Kh-Kh. Nugmanov, I.Yu. Aleksanyan, M.A.S. Barzola, L.M. Titova, Z.M. Arabova. Extraction of Chlorophyll From Technologically Prepared Spinach Leaves  International Journal of Engineering Trends and Technology, 69(4),100-106.

Abstract
The purpose of this research is to improve the processes of obtaining chlorophyll extract from technologically prepared spinach leaves, which will eventually produce fat-soluble chlorophyll paste. According to this objective, the authors solved a number of problems. In particular, they selected rational technological solutions for preparing plant raw materials in order to extract photosynthetic pigments from them. The authors also identified specific features of the use of ultrasound at this stage, which resulted in the choice of rational temperature conditions when it affects plant material. Additionally, the identified kinetic regularities of the extraction process are presented, and a rational approach to extracting the target component from the object of study is proposed on their basis. As a result, due to the analysis of the structures of extraction plants for processes in the solid-liquid system, the article provides practical recommendations for implementing the research results. Namely, a two-section original installation for obtaining alcohol extract with the specified indicators of the final volume concentration of the target component in it is proposed.

Reference
[1] Aktas, E.T., Yildiz, H., Effects of electroplasmolysis treatment on chlorophyll and carotenoid extraction yield from spinach and tomato. Journal of food engineering, 106(4)(2011) 339-346.
[2] Aleksanyan, I.Yu., Buynov, A.A., Vysokointensivnaya sushka pishchevykh produktov. Penosushka. Teoriya. Praktika. Modelirovaniye: monografiya [High-intensity food drying. Foam dryer. Theory. Practice. Modeling: Monograph]. Astrakhan: Astrakhan State Technical University, 380(2004) (In Russ).
[3] Azmir, J., Zaidul, I.S.M., Rahman, M.M., Sharif, K.M., Mohamed, A., Sahena, F., Jahurul, M.H.A., Ghafoor, K., Norulaini, N.A.N., Omar, A.K.M., Techniques for extraction of bioactive compounds from plant materials: A review. Journal of food engineering, 117(4)(2013) 426-436.
[4] Bedoux, G., Hardouin, K., Marty, C., Taupin, L., Vandanjon, L., Bourgougnon, N., Chemical characterization and photoprotective activity measurement of extracts from the red macroalga Solieria chordalis. Botanica marina, (2014) 291-301.
[5] Bokuchayeva M.A., Pruidze G.N., Ulyanova M.S., Biokhimiya proizvodstva rastitel’nykh krasiteley [Biochemistry of plant dye production]. Tbilisi: Mitsniereba, 96(1976) . (In Russ).
[6] Buckenhuskes, H., Glaus, M., Uhtercuchunger zur Stabiiitat Von Anthocyanen oms Rotkraut. Ernar. Nutr.,12(10)(1988) 620-625.
[7] Cha, K.H., Kang, S.W., Kim, C.Y., Um, B.H., Na, Y.R., Pan, C.H., Effect of Pressurized Liquids on Extraction of Antioxidants from Chlorella vulgaris. Journal of agricultural and food chemistry, 58(8)(2010) 4756-4761.
[8] Duan, W.H.; Cao, S. (2016). Determination of the Liquid Hold-up Volume and the Interface Radius of an Annular Centrifugal Contactor using the Liquid-Fast-Separation Method. Chemical engineering communications, 203(4)(2016) 548-556.
[9] Golubev, V.N., Pilipenko, L.N., Kobeleva, S.M., Grishin, M.A., Zelenskaya, L.D., Spinach drying method. USSR 1450811. (In Russ).
[10] Gülay, Ö., Seda, E.B. (2015). Enzyme-assisted extraction of stabilized chlorophyll from spinach. Food Chemistry, 176(1989) 152-157.
[11] Heaton, J.W., Marangoni, A.G., Chlorophyll degradation in processed foods and senescent plant tissues. Trends in food science & technology, 7(1)(1996) 8-15.
[12] Hernandez, Y., Lobo, M.G., Gonzalez, M., Factors affecting sample extraction in the liquid chromatographic determination of organic acids in papaya and pineapple. Food Chemistry, 114(2)(2009) 734-741.
[13] Humphrey, A.M., Chlorophyll. Food Chemistry, 5(1)(1980) 57-67.
[14] Katsernikova, N.V., Ilyina, N.G., Kazankova, O.A., et al., Method for producing pigment additives from plant materials. Russia patent RU 2154075. (In Russ)., (2000).
[15] Koca, N., Karadeniz, F., Burdurlu, H.S., Effect of pH on chlorophyll degradation and color loss in blanched green peas. Food Chemistry, 100(2)(2007) 609-615.
[16] Limareva, N.S., Donchenko, L.V., Funktsionalnyye pektinoso-derzhashchiye napitki na osnove shpinata [Functional beverages containing pectin based on spinach]. Sovremennaya nauka i innovatsii [Modern science and innovation], 4(2016) 99-104. (In Russia).
[17] Marzorati, S., Schievano, A., Ida, A., Verotta, L., Carotenoids, chlorophylls, and phycocyanin from Spirulina: supercritical CO2 and water extraction methods for added value products cascade. Green chemistry, 22(1)(2020) 187-196.
[18] Mukatova, M.D., Kabanin, M.I., Salieva, A.R., Method for producing chlorophyll from higher aquatic plants. Russia patent RU 2496813. (In Russ).,(2013).
[19] Panin, A.S., Skverchak, V.D., Ekspress-metod opredeleniya koeffitsiyenta teploprovodnosti pastoobraznykh i melkodispersnykh materialov [Express method for determining the coefficient of thermal conductivity of pasty and finely dispersed materials]. Izvestiya vuzov SSSR. Pishchevaya tekhnologiya [Proceedings of the universities of the USSR. Food technology], 1(1974) 140-143. (In Russia).
[20] Roberts, J.L., Moreau, R., Functional properties of spinach (Spinacia oleracea L.) phytochemicals and bioactives. Food Funct., 7(8)(2016) 3337-3353.

Keywords
Chlorophyll, extraction, ultrasound, process kinetics, kinetic coefficients.