Synthesis and Research of Sorbent Based on Sodium Metalsilicate and Thiourea

Synthesis and Research of Sorbent Based on Sodium Metalsilicate and Thiourea

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© 2022 by IJETT Journal
Volume-70 Issue-11
Year of Publication : 2022
Authors : Turaev Kh, Gafforova Sh., Dzhalilov A, Sottikulov E, Soatov S
DOI : 10.14445/22315381/IJETT-V70I11P210

How to Cite?

Turaev Kh, Gafforova Sh., Dzhalilov A, Sottikulov E, Soatov S, "Synthesis and Research of Sorbent Based on Sodium Metalsilicate and Thiourea," International Journal of Engineering Trends and Technology, vol. 70, no. 11, pp. 99-105, 2022. Crossref, https://doi.org/10.14445/22315381/IJETT-V70I11P210

Abstract
The purpose of this study is to synthesize and research a new type of sorbent based on thiourea and sodium metasilicate, which has a wide range of applications and has selective sorption properties due to the presence of the thio group in the molecule and the presence of silicon in its composition. During the synthesis of the sorbent, 60 g of thiourea and 100 g of sodium metasilicate were taken from an aqueous solution and heated in a water bath at a temperature of 90 °C. The duration of the reaction is 25-30 minutes, after 30 minutes the reaction mass cools down to room temperature, and after 24 hours the mass comes to a brittle state in the form of a gel. The resulting mass was crushed to a size of 1 mm and thermally treated at a temperature of 200 °C. The synthesized sorbent was thoroughly washed in distilled water and stored at 105°С-110°С until the mass reached a constant state. The yield of the reaction product is 91%. The reaction mechanism of the organ hybrid sorbent based on thiourea and sodium metasilicate was compared and the IR-spectra of the initial reagents and the obtained product were analyzed and the reaction mechanism was proposed. At the same time, the results of the thermal analysis of the obtained sorbent and SEM analysis of the sorbent were presented.

Keywords
Corbent, Thiomochevine, Sodium metasilicate, IR spectrum, Thermogravimetric curve, Mass loss, Scanning electron microscopy.

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